Cookies Policy
X

This site uses cookies. By continuing to browse the site you are agreeing to our use of cookies.

I accept this policy

Find out more here

Synthesis of Tin Oxide Hydrate (SnO2 ˙ xH2O) Gel and its Effects on the Hydrothermal Preparation of BaSnO3 Powders

No metrics data to plot.
The attempt to load metrics for this article has failed.
The attempt to plot a graph for these metrics has failed.
The full text of this article is not currently available.

Brill’s MyBook program is exclusively available on BrillOnline Books and Journals. Students and scholars affiliated with an institution that has purchased a Brill E-Book on the BrillOnline platform automatically have access to the MyBook option for the title(s) acquired by the Library. Brill MyBook is a print-on-demand paperback copy which is sold at a favorably uniform low price.

This Article is currently unavailable for purchase.
Add to Favorites
You must be logged in to use this functionality

Cover image Placeholder

Perovskite-type BaSnO3 powders with a particle size of 30–60 nm have been prepared from tin oxide hydrate (SnO2 ˙ xH2O) gel via the hydrothermal synthesis route. The reactivity of the synthesized SnO2 ˙ xH2O was found to be dependent on the pH value of the mixture of tin chloride and the ammonia solution. The most reactive SnO2 ˙ xH2O gel was obtained at a pH value near 2. The hydrothermal products derived from this reactive gel were characterized with thermograrimetric/differential thermal analysis, Fourier transform infrared spectrometry, X-ray diffraction and high-resolution scanning electron microscopy. The BaSn(OH)6 phase in the as-prepared powder was found to convert into an amorphous phase other than into the BaSnO3 phase. The BaSnO3 powder crystallizing from the amorphous phase at 260°C for 4 h has better sintering properties than the commercial one.

Affiliations: 1: Leibniz-Institut fuer Neue Materialien gGmbH, Im Stadtwald, Gebaeude D2 2, 66123 Saarbruecken, Germany;, Email: Wensheng.Lu@inm-gmbh.de; 2: Universitaet des Saarlandes, Lehrstuhl fuer Neue Materialien, Beethovenstraße Zeile 4, 66125 Saarbruecken-Dudweiler, Germany

10.1163/156855208X291666
/content/journals/10.1163/156855208x291666
dcterms_title,pub_keyword,dcterms_description,pub_author
10
5
Loading
Loading

Full text loading...

/content/journals/10.1163/156855208x291666
Loading

Data & Media loading...

http://brill.metastore.ingenta.com/content/journals/10.1163/156855208x291666
Loading

Article metrics loading...

/content/journals/10.1163/156855208x291666
2017-07-28

Sign-in

Can't access your account?
  • Key

  • Full access
  • Open Access
  • Partial/No accessInformation