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Synthesis and Characterization of MSU Molecular Sieve Catalysts Obtained by Direct Incorporation of Platinum and 12-tungstophosphoric Acid H3PW12O40

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Direct incorporation of platinum (Pt) and 12-tungstophosphoric acid H3PW12O40 (HPW) into mesoporous MSU-type silica was achieved by using a mixture of cationic and non-ionic surfactants, such as cetyltrimethylamonium and Triton (TX-100). Various amounts of Pt (0.3–7 wt%) and HPW (9–49 wt%) were incorporated, and the obtained materials were characterized by X-ray diffraction, chemical and thermal analyses, electron microscopy, N2 adsorption–desorption measurements and solid-state 31P nuclear magnetic resonance spectroscopy.

Affiliations: 1: Laboratoire de Matériaux à Porosité Contrôlée, UMR 7016, ENSCMu, UHA, 3 rue Alfred Werner, 68093 Mulhouse Cedex, France; Laboratoire de Chimie Analytique, Matériaux, Surfaces et Interfaces (CHAMSI), Département de Chimie, Faculté des Sciences, Section 1, Université Libanaise, Hadeth, Mont-Liban, Beyrouth, Lebanon; 2: Laboratoire de Chimie Analytique, Matériaux, Surfaces et Interfaces (CHAMSI), Département de Chimie, Faculté des Sciences, Section 1, Université Libanaise, Hadeth, Mont-Liban, Beyrouth, Lebanon; Institut de Chimie des Surfaces et Interfaces (ICSI-CNRS), UPR 9096 15, Rue Jean Starcky, BP 2488, 68057 Mulhouse Cedex, France; 3: Laboratoire Gestion des Risques et Environnement, EA 2334, UHA, 25 rue de Chemnitz, 68200 Mulhouse, France; 4: Laboratoire de Chimie Analytique, Matériaux, Surfaces et Interfaces (CHAMSI), Département de Chimie, Faculté des Sciences, Section 1, Université Libanaise, Hadeth, Mont-Liban, Beyrouth, Lebanon

10.1163/156855208X293790
/content/journals/10.1163/156855208x293790
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/content/journals/10.1163/156855208x293790
2008-03-01
2016-12-09

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