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Mechanochemical effects on pulverization of a Bi-Pb-Sr-Ca-Cu-O Superconductor

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—Mechanochemical effects on the pulverization of Bi-Pb-Sr-Ca-Cu-O superconductor powder were examined. Pulverization of superconducting was carried out with wet operation using a media agitation type mill. Particle size was reduced to submicron size accompanied with a deterioration of crystallinity. Superconducting properties decreased with damaging of the crystal structure as the result of pulverization. Heat treatment of ground powders of high-Tc phase with prolonged grinding time promoted phase transition from a high-Tc phase to a low-Tc phase. This phenomenon revealed phase stability in this system with accumulated crystal strain in ground powder under heating conditions.

Affiliations: 1: Government Industrial Research Institute, Nagoya, 1-1 Hirate-cho, Kita-ku, Nagoya 462, Japan; 2: Saga Ceramics Research Laboratory, 3100-5 Chubu-otu, Arita town, Saga Prefecture 844, Japan


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