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A basic study on the solid-state nitriding of aluminum by mechanical alloying using a planetary ball mill

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Nitrogen dispersed amorphous aluminum powders were synthesized by high energy grinding using a planetary ball mill under N2 atmosphere at room temperature. The modes of amorphization and recrystallization during the grinding were investigated by means of X-ray diffraction, scanning electron microscopy and transmission electron microscopy. The grinding process can be classified into three stages, i.e. agglomeration, disintegration and homogenization. During the disintegration stage, an amorphous phase was formed and N2 was supposed to diffuse into the aluminum. Recrystallization of N2 dispersed amorphous aluminum powders was also studied. By annealing the final ground product in air and in vacuum at 1373 K for 3600 s, the particles were recrystallized to A1N/A12O3 and AlN/Al composite, respectively.

Affiliations: 1: Korea Mining Promotion Corporation, 686-48, Shin Dae Bang-dong, Dong Jak-ku, Seoul, Korea; 2: Material Handling and Characterization Division, National Institute for Resources and Environment, 16-3 Onogawa, Tsukuba, Ibaraki 305, Japan; 3: Material Processing Department, National Institute for Resources and Environment, 16-3 Onogawa, Tsukuba, Ibaraki 305, Japan


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