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Formation of ceria partially stabilized zirconia nanocrystals by laser evaporation-condensation

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Sintered CeO2-ZrO2 (1 : 9 molar ratio) targets were subject to CO2 laser ablation (1600 W for 8 s in air) regarding alloying and phase transformation of the fluorite-type condensates for potential engineering applications. Analytical electron microscopy indicated the CeO2-ZrO2 solid solution condensates contain tetragonal precipitates in the cubic phase matrix and are generally spherical in shape. On the other hand, dendritic particles with curved vicinal {~ 111} surfaces were also formed, due to the combined effects of Wulff shape, constitutional supercooling and cellular growth along <110>. The relatively large particles have a clear Si (impurity)-rich amorphous shell indicating a vapor-liquid-solid formation mechanism.

Affiliations: 1: Institute of Materials Science and Engineering, National Sun Yat-sen University, Kaohsiung, Taiwan 804, ROC


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