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Microwave synthesis, characterization and catalytic properties of titanium-incorporated ZSM-5 zeolite

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Titanium-incorporated ZSM-5 zeolites (Si/Al = 50–200 and Si/Ti = 70) were successfully synthesized in a one-step sol–gel process under microwave irradiation. The characteristics of Ti-ZSM-5 zeolites were investigated using X-ray power diffraction, UV/Vis-DRS, FT-IR spectroscopy and solid-state 27Al-NMR to monitor the physico-chemical properties. Simultaneously, the acidic properties were characterized by the NH3-TPD profile. The characterization results revealed that the Ti4+ and Al3+ ions were well incorporated into the framework of Ti-ZSM-5 zeolite. The prepared zeolite was moderately active but selective in the dehydration of methanol to dimethyl ether.

Affiliations: 1: Catalysis Center for Molecular Engineering, Korea Research Institute of Chemical Technology (KRICT), P.O. Box 107, Yuseong, Daejeon 305-600, South Korea; 2: Department of Chemistry, Inha Univertisy, Incheon 402-751, South Korea; 3: Department of Fine Chemicals Engineering & Chemistry, Chungnam National University, Daejeon 305-764, South Korea


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