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Evaluation of microstructures and properties of bulk mesoporous silica

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Synthesis of mesoporous MCM-type bulks prepared by hydrothermal hot-pressing (HHP) method using MCM-type mesoporous powder was attempted. Scanning electron microscopy (SEM), bulk density measurement, N2 adsorption–desorption isotherms and formaldehyde adsorption test have been employed to characterize the bulky products. As a result, we succeeded in preparing a dense and strong mesoporous bulks with high BET over 1000 m2/g through the hydrothermal hot-pressing method under appropriate conditions.

Affiliations: 1: Osaka Prefecture University, 1-1, Gakuen-cho, Naka-ku, Sakai, Osaka 599-8531, Japan;, Email:; 2: Osaka Prefecture University, 1-1, Gakuen-cho, Naka-ku, Sakai, Osaka 599-8531, Japan; 3: Tokyo Institute of Technology, 4259, Nagatsuta-cho, Midori-ku, Yokohama 226-8503, Japan; 4: Hosei University, 4342, Aihara-cho, Machida, Tokyo 194-0298, Japan


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