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Esr and Cidep Studies of the Photooxidation of Phenols in Single Crystals and in Solutions

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Photooxidation of single crystals of 2,6-di-tert-butyl-4-methylphenol and 2,6-di-tert-butylphenol, respectively, led to localized pair-wise trapping of triplet phenoxyl radical pairs. Electron ejection is not implicated in the primary photooxidation of phenols in single crystals, but in liquid solutions time-resolved CIDEP observations for the 2,4,6-tritert-butylphenol in hexaftuorobenzene suggest an initial formation of a phenol radical cation from the photoexcited triplet state.

Affiliations: 1: Department of Chemistry Queen's University Kingston, Canada K7L 3N6

10.1163/156856789X00302
/content/journals/10.1163/156856789x00302
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/content/journals/10.1163/156856789x00302
2017-10-23

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