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Homolytic Cleavage of the β-Ether Bond in Phenolic β-O-4 Structures in Wood Lignin and in Guaiacylglycerol-β-Guaiacyl Ether

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The degradation of guaiacylglycerol-β-guaiacyl ether and lignin in spruce wood was studied in order to investigate the extent of homolytic reactions on heating with dioxane: water media ("mild hydrolysis"). The degradation reactions were studied at different temperatures, reaction times and pH-values. The results clearly show that extensive cleavage of phenolic β-ethers occur under the conditions prevailing during heating in dioxane:water media. Homolytic cleavage of phenolic β-ethers should therefore be considered in interpretations of results from "mild hydrolysis" of lignin.

Affiliations: 1: STFI Swedish Pulp and Paper Research Institute, Box 5604, S-114 86 Stockholm, SWEDEN; 2: Department of Organic Chemistry, Chalmers University of Technology, S-412 96 Göteborg, SWEDEN

10.1163/156856795X00297
/content/journals/10.1163/156856795x00297
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/content/journals/10.1163/156856795x00297
1995-01-01
2016-12-05

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