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Line Widths in Nitroxides

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The 2,5-di-tert-butyl-3,4-dimethoxycarbonyl-pyrryloxyl radical has the smallest line-width and the smallest nitrogen hyperfine splitting reported for a stable nitroxide. The influence of long range proton splittings was shown by selective and total deuteriation. As expected on theoretical grounds, line widths and nitrogen hyperfine splitting are correlated.

Affiliations: 1: Nycomed Innovation AB, Ideon Malmö, S-221 00, Malmö, Sweden; 2: Ecole Normale Supérieure, Département de Chimie (URA CNRS 1679), 24 rue Lhomond, F-7523 Paris Cedex 05, France


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