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Additional Effects of Urea and Hexamethylenetetramine on Preparation and Acidic Properties of Aluminum Polyphosphates

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Aluminum polyphosphate was prepared from aluminum nitrate solution and sodium polyphosphate solution with cation exchange resin in the molar ratio of Al/P = 1/3. Urea and hexamethylenetetramine were added in this preparation process. The thermal behavior of the obtained phosphates was analyzed by differential thermal analyses, X-ray diffraction, and Fourier transform infrared spectroscopy. Furthermore, these materials and their thermal products were estimated by specific surface area, pore size distribution, particle size distribution, acid strength, amount of acidic sites, and adsorption of trimethylamine.

Affiliations: 1: Division of Inorganic Materials Chemistry, Chemical Resource Laboratory, Tokyo Institute of Technology, 4259-R1-21, Nagatsuta, Midori, Yokohama, 226-8503, Japan; 2: Department of Applied Chemistry, Faculty of Science and Engineering, Ritsumeikan University, 1-1-1, Nojihigashi, Kusatsu, Shiga 525-8577, Japan; 3: Department of Materials Science, Yonago National College of Technology, 4448, Hikona-cho, Yonago, Tottori 683-8502, Japan

10.1163/157361109787959877
/content/journals/10.1163/157361109787959877
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/content/journals/10.1163/157361109787959877
2009-04-01
2016-12-04

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